HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13361751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | (2R,3S,4S,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 3037556 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 13361751 | HCID 13361751 | — |
Reaction Steps
60 g of D-galactose were suspended in 330 ml of isopropanol and 170 ml of water and heated to 50°. After addition of 90 g of stearylamine, the mixture was stirred until all the amine had gone into solution. On cooling, the glycosylamine crystallised out. The solid material was filtered off with suction, washed consecutively with ethanol and with ether and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04683222 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-4c4115704f1649888cd597d0e18b6ce4 |
| Source note | uspto-grants-1987_07 |