Tetradecylamine → HCID 54500416, compound

HRID 2119155Notes

Reaction equation

HRID 2119155 reaction equation
O=[CH:2][C@H:3]([C@H:5]([C@@H:7]([C@@H:9]([CH2:11][OH:12])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:13]([NH2:27])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[CH2:13]([NH:27][CH:2]1[O:10][C@H:9]([CH2:11][OH:12])[C@@H:7]([OH:8])[C@H:5]([OH:6])[C@@H:3]1[OH:4])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

3

Reactant 2

HCID 16217TetradecylamineHCID 161658Demannose

Product 1

HCID 54500416HCID 54500416, compound

Procedure

20 g of D-mannose and 35 g of tetradecylamine were reacted as described in Example 44 to give N-tetradecylmannopyranosylamine. In a second reaction step, the glycosylamine (7.5 g) was reacted with 6.0 g of oleoyl chloride as described in Example 11 to give the glycosylamide.

Sources & evidence

ORD record
ord-1f84834db48f461ab830950c50099ffc
Source dataset
uspto-grants-1987_07
Patent number
US04683222

Reaction notes

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