HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrogen → HCID 14010414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 4,4'-Dihydroxyazobenzene | HCID 101245 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14010414 | HCID 14010414 | — |
Reaction Steps
1 g (0.0047 mole) of 4,4'-dihydroxyazobenzene and 2 g (0.016 mole) of pivaloyl chloride was stirred in 20 mls of pyridine for 24 hrs. at room temperature. The solvent was blown off under a stream of N2. Water was added and the crude product filtered and recrystallized from ethanol; 1.5 g (83%) yield. M.P.~185°-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04683241 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-f5109f00c0894e8dbcd746555f01a02b |
| Source note | uspto-grants-1987_07 |