HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzophenone → 4-Benzoylphenyl 2-methylpropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzophenone | HCID 14347 | — |
| Reactant | Isobutyryl chloride | HCID 62325 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-Benzoylphenyl 2-methylpropanoate | HCID 14010383 | — |
Reaction Steps
To a solution of 8.5 g of 4-hydroxybenzophenone in 75 ml of dry pyridine 6.75 ml of isobutyric chloride was added at 0°~10° C. The reaction mixture was allowed to stand at 25° C. for 2 h, poured into ice water. The precipitate was collected by suction and recrystallized from ethanol; M.P.~69°-69.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04683241 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-867bdbba31fd46b3b2e18b50ec420352 |
| Source note | uspto-grants-1987_07 |