HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaminophen → 4,4'-[Decane-1,10-diylbis(oxy)]dianiline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaminophen | HCID 1983 | — |
| Reactant | 1,10-Dibromodecane | HCID 221483 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Product | 4,4'-[Decane-1,10-diylbis(oxy)]dianiline | HCID 13580685 | — |
Reaction Steps
Tetrabutylammonium bromide was used as the phase transfer catalyst. It was added to the contents of the flask immediately following addition of the second portion of the 1,10-dibromodecane. The amount of catalyst was 0.50 grams, or 2.5 parts per hundred parts of 4-acetamidophenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04683333 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-1e0a815c3e5140b39a483d156fd3e4c6 |
| Source note | uspto-grants-1987_07 |