HCID 11732192, compound → HCID 70112951, compound

HRID 2119318Notes

Reaction equation

HRID 2119318 reaction equation
[Cl-].C1([P+](C2C=CC=CC=2)(C2C=CC=CC=2)[CH2:9][C:10]2[CH:11]=[N:12][C:13]([CH3:16])=[CH:14][CH:15]=2)C=CC=CC=1.[C:29]1(=[O:41])[C:38]2[C:33](=[CH:34][CH:35]=[CH:36][CH:37]=2)[C:32]([CH:39]=O)=[N:31][NH:30]1.N1C=CC=C(/C=C\C2C3C(=CC=CC=3)C(=O)NN=2)C=1>>[CH3:16][C:13]1[N:12]=[CH:11][C:10](/[CH:9]=[CH:39]\[C:32]2[C:33]3[C:38](=[CH:37][CH:36]=[CH:35][CH:34]=3)[C:29](=[O:41])[NH:30][N:31]=2)=[CH:15][CH:14]=1

Participants

4

Reactant 3

HCID 11732192HCID 11732192, compoundHCID 157289693,4-Dihydro-4-oxo-1-phthalazinecarboxaldehydeHCID 70111827HCID 70111827, compound

Product 1

HCID 70112951HCID 70112951, compound

Procedure

Prepared by Wittig reaction of triphenyl-(6-methylpyridin-3-yl-methyl)phosphonium chloride and phthalazin-1(2H)-one-4-carbaldehyde as described in expl. 4d): HPLC5-40 tR=11.7/12.2.

Sources & evidence

ORD record
ord-27cea93690ff406baee7f304f82c18db
Source dataset
uspto-grants-2004_02
Patent number
US06686347B2

Reaction notes

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