Ethanolamine → HCID 69891131, compound

Participants

Reaction Conditions

Reaction Steps

Crude product from (a) was diluted up in anhydrous THF (1 mL) in a dry environment and then cooled to ˜0° C. To this solution was added ethanolamine (1 mL of a 0.2 M solution in dry THF). This was allowed to warm to room temperature while stirring overnight. Concentration in vacuo, followed by hydrolysis of the ester as described in part (c) of Example 5 gave the title compound.

Provenance & Evidence