HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → HCID 23440774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | 6-Methoxy-1-[4-(phenylmethoxy)benzyl]-1,2,3,4-tetrahydroisoquinoline | HCID 12950735 | — |
| Product | HCID 23440774 | HCID 23440774 | 53% |
Reaction Steps
The title compound was prepared as described in Example 14.C, using 6-methoxy-1-[4-(phenylmethoxy)benzyl]-1,2,3,4-tetrahydroisoquinoline (0.5 g, 1.39 mmol) and cyclohexanone (0.588 g. 6.0 mmol) to provide the title compound (0.324 g, 53% yield): ES−MS (m/z) 442 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686351B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-c3fd0bdf3cc143aaab2ca24905151f7d |
| Source note | uspto-grants-2004_02 |