HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 9819479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Reactant | 3-(1,2,3,5,8,8a-hexahydro-7-indolizinyl)-1H-5-Azaindole | HCID 10130974 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9819479 | HCID 9819479 | — |
Reaction Steps
from 3-(1,2,3,5,8,8a-hexahydro-7-indolizinyl)-1H-5-Azaindole (10 mg, 0.0418 mmol), benzoyl chloride (13 μL, 0.12 mmol) and 1M NaN(TMS)2 (100 μL, 0.10 mmol) in THF (1 mL) at RT.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686374B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-0d34f997dd34462390a3388ffca07ce1 |
| Source note | uspto-grants-2004_02 |