HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloro-2-isothiocyanatobenzene → HCID 22288828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloro-2-isothiocyanatobenzene | HCID 123239 | — |
| Reactant | 2,3-Diaminophenol | HCID 579937 | — |
| Product | HCID 22288828 | HCID 22288828 | 61% |
Reaction Steps
1.0 equivalent of 2,6-dichlorophenyl isothiocyanate was treated with 1.0 equivalent of 2,3-diaminophenol and heated to reflux for 1 h. After cooling to RT, the precipitate was filtered off with suction, washed with ether, and dried. The desired thiourea was obtained in a yield of 61%. M.p.: 202-204° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686384B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-997e66cbea5048db835b116ade979575 |
| Source note | uspto-grants-2004_02 |