1-(4-Methyl-3-pyridinyl)ethanone → 2-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one hydrobromide

HRID 2119585Notes

Reaction equation

HRID 2119585 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[C:8](=[O:10])[CH3:9].[BrH:11].BrBr>>[BrH:11].[Br:11][CH2:9][C:8]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:2]=1[CH3:1])=[O:10]

Participants

3

Reactant 2

HCID 109424811-(4-Methyl-3-pyridinyl)ethanoneHCID 86584092HBr bromine

Product 1

HCID 227309902-Bromo-1-(4-methylpyridin-3-yl)ethan-1-one hydrobromideYield 85%

Procedure

The title compound was synthesised according to Example E 1-(4-methyl-pyridin-3-yl)-ethanone and HBr/bromine in 85% yield as grey solid. MS (m/e): 214.0 (M+H, 100%).

Sources & evidence

ORD record
ord-ce5d20f190254330a78ff80bfabda02d
Source dataset
uspto-grants-2004_02
Patent number
US06686381B2

Reaction notes

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