HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12985698, compound → HCID 23442493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12985698 | HCID 12985698 | — |
| Reactant | HCID 23442346 | HCID 23442346 | — |
| Reactant | HCID 23442370 | HCID 23442370 | — |
| Reactant | HCID 23442408 | HCID 23442408 | — |
| Product | HCID 23442493 | HCID 23442493 | — |
Reaction Steps
A mixture of 9-chloro-8-isopropyl-1-methyl-1H-pyrazolo[4,3-b]quinoline and 9-chloro-6-isopropyl-1-methyl-1H-pyrazolo[4,3-b]quinoline (EXAMPLE 10, step 2) was treated according to the procedure of step 3 in EXAMPLE 3 instead of 9-chloro-6-fluoro-1-methyl-1H-pyrazolo[4,3-b]quinoline. The title compound and 6-isopropyl-1-methyl-1,4-dihydro-9H-pyrazolo[4,3-b]quinolin-9-one were separable by column chromatography on silica gel eluting with methanol/dichloromethane (1:30).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686373B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-da2f28772ea247488d6cc080cde89347 |
| Source note | uspto-grants-2004_02 |