HCID 23442373, compound → HCID 9967020, compound
Reaction equation
[Cl:1][C:2]1[CH:26]=[CH:25][CH:24]=[CH:23][C:3]=1[CH2:4][C:5]1[CH:6]=[CH:7][C:8]([N+:20]([O-])=O)=[C:9]([C:11]([C:13]2[N:17]([CH3:18])[N:16]=[CH:15][C:14]=2I)=[O:12])[CH:10]=1.ClC1C=CC(CC2C=CC([N+]([O-])=O)=C(C(C3N(C)N=CC=3I)=O)C=2)=CC=1>>[Cl:1][C:2]1[CH:26]=[CH:25][CH:24]=[CH:23][C:3]=1[CH2:4][C:5]1[CH:6]=[CH:7][C:8]2[NH:20][C:14]3[CH:15]=[N:16][N:17]([CH3:18])[C:13]=3[C:11](=[O:12])[C:9]=2[CH:10]=1Participants
3
Procedure
The title compound was prepared according to the procedure of step 5 in EXAMPLE 13 using [5-(2-chlorobenzyl)-2-nitrophenyl](4-iodo-1-methyl-1H-pyrazol-5-yl)methanone (EXAMPLE 15, step 3), instead of [5-(4-chlorobenzyl)-2-nitrophenyl](4-iodo-1-methyl-1H-pyrazol-5-yl)methanone.
Sources & evidence
- ORD record
- ord-f2a66be90ec846dd81eec7a81a868bfc
- Source dataset
- uspto-grants-2004_02
- Patent number
- US06686373B2
Reaction notes
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