HCID 23442307, compound → HCID 9967020, compound
Reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[Cl:15])=[CH:4][C:3]=1[C:16]([C:18]1[N:22]([CH3:23])[N:21]=[CH:20][C:19]=1I)=[O:17].NC1C=CC(CC2C=CC(Cl)=CC=2)=CC=1C(C1N(C)N=CC=1I)=O>>[Cl:15][C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=1[CH2:8][C:5]1[CH:6]=[CH:7][C:2]2[NH:1][C:19]3[CH:20]=[N:21][N:22]([CH3:23])[C:18]=3[C:16](=[O:17])[C:3]=2[CH:4]=1Participants
3
Procedure
The title compound was prepared according to the procedure of step 6 in EXAMPLE 13 using [2-amino-5-(2-chlorobenzyl)phenyl](4-iodo-1-methyl-1H-pyrazol-5-yl)methanone (EXAMPLE 15, step 4), instead of [2-amino-5-(4-chlorobenzyl)phenyl](4-iodo-1-methyl-1H-pyrazol-5-yl)methanone.
Sources & evidence
- ORD record
- ord-ec98c32a32b244218c599f0eb6e52683
- Source dataset
- uspto-grants-2004_02
- Patent number
- US06686373B2
Reaction notes
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