HCID 23442343, compound → HCID 10267948, compound

HRID 2119630Notes

Reaction equation

HRID 2119630 reaction equation
[CH3:1][O:2][C:3]1[CH:27]=[CH:26][C:6]([CH2:7][C:8]2[CH:9]=[CH:10][C:11]([N+:23]([O-])=O)=[C:12]([CH:14]([C:16]3[N:20]([CH3:21])[N:19]=[CH:18][C:17]=3I)[OH:15])[CH:13]=2)=[CH:5][CH:4]=1.ClC1C=CC(CC2C=CC([N+]([O-])=O)=C(C(C3N(C)N=CC=3I)O)C=2)=CC=1>>[CH3:1][O:2][C:3]1[CH:27]=[CH:26][C:6]([CH2:7][C:8]2[CH:9]=[CH:10][C:11]3[NH:23][C:17]4[CH:18]=[N:19][N:20]([CH3:21])[C:16]=4[C:14](=[O:15])[C:12]=3[CH:13]=2)=[CH:5][CH:4]=1

Participants

3

Procedure

The title compound was prepared according to the procedure of step 4 in the EXAMPLE 13 using [5-(4-methoxybenzyl)-2-nitrophenyl](4-iodo-1-methyl-1H-pyrazol-5-yl)methanol (EXAMPLE 16, step 2), instead of [5-(4-chlorobenzyl)-2-nitrophenyl](4-iodo-1-methyl-1H-pyrazol-5-yl)methanol.

Sources & evidence

ORD record
ord-241d75b131ac4f938a08fce0cdf76c6b
Source dataset
uspto-grants-2004_02
Patent number
US06686373B2

Reaction notes

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