HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethylpropyl carbonochloridate → HCID 9955140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethylpropyl carbonochloridate | HCID 3352185 | — |
| Reactant | 2'-(Aminomethyl)-N-(2-phenylethyl)[1,1'-biphenyl]-2-carboxamide | HCID 15509384 | — |
| Product | HCID 9955140 | HCID 9955140 | — |
Reaction Steps
From 0.45 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid phenethylamide (precursor 5a) and neopentyl chloroformate, according to the general working procedure followed by extraction with EA and purification by flash chromatography 156 mg of 2′-(2,2-dimethylpropoxycarbonylaminomethyl)biphenyl-2-carboxylic acid phenethylamide were obtained. MS (ES+): m/e=445 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686395B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-e8d07a65e8c64e04be0b5f192beefe9a |
| Source note | uspto-grants-2004_02 |