Benzo(d)thiazol-2-amine → HCID 9945577, compound

HRID 2119791Notes

Reaction equation

HRID 2119791 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH3:11])=[C:6]([N:8]=[C:9]=[S:10])[CH:7]=1.[NH2:12][C:13]1[S:14][C:15]2[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=2[N:17]=1>>[S:14]1[C:15]2[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=2[N:17]=[C:13]1[NH:12][C:9]([NH:8][C:6]1[CH:7]=[C:2]([Cl:1])[CH:3]=[CH:4][C:5]=1[CH3:11])=[S:10]

Participants

3

Reactant 2

HCID 8706Benzo(d)thiazol-2-amineHCID 295195-Chloro-2-methylphenyl isothiocyanate

Product 1

HCID 9945577HCID 9945577, compoundYield 31.1%

Procedure

Prepared using Method A from 5.0 g (27.2 mmol) of 5-chloro-2-methyl-phenyl isothiocyanate and 3.90 g (26 mmol) of 2-aminobenzothiazole to give 2.7 g of title compound as a white fluffy solid (30% yield).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-02221d8faefb4ddf9f314b04c412b7fb
Source dataset
uspto-grants-2004_02
Patent number
US06686476B2

Reaction notes

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