HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methylphenyl isothiocyanate → HCID 178425388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methylphenyl isothiocyanate | HCID 29519 | — |
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Product | HCID 178425388 | HCID 178425388 | 66% |
Reaction Steps
Prepared using Method A from 5.5 g (30.1 mmol) of 5-chloro-2-methyl-phenyl isothiocyanate and 2.5 g (30.1 mmol) of 3-amino-1H-pyrazole to give 5.3 g of title compound as a white solid (66% yield, m.p. 221-222° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686476B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ac885b7c6bb947e38337761233b03ee5 |
| Source note | uspto-grants-2004_02 |