HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonic acid, 3-nitro-, (2R)-2-oxiranylmethyl ester → HCID 22147730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonic acid, 3-nitro-, (2R)-2-oxiranylmethyl ester | HCID 146513 | — |
| Reactant | HCID 22147703 | HCID 22147703 | — |
| Product | HCID 22147730 | HCID 22147730 | 78.4% |
Reaction Steps
1-Fluoro-5-hydroxycarbazole (25 mg, 0.124 mmol) and (2R)-(−)-glycidyl 3-nitrobenzenesulfonate, (32 mg, 0.124 mmol) were converted to 25 mg of the title compound substantially in accordance with the procedure of Preparation 122. Yield: 65%. 1H NMR. MS(FD).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686372B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-7ddff57411864d67a5573e8bf557908d |
| Source note | uspto-grants-2004_02 |