Acetamidine monohydrochloride → HCID 23440980, compound

HRID 2119968Notes

Reaction equation

HRID 2119968 reaction equation
CN([CH:4]=[C:5]1[C:11](=O)[C:10]2[CH:13]=[C:14]([CH3:17])[CH:15]=[CH:16][C:9]=2[NH:8][C:7](=[O:18])[CH2:6]1)C.Cl.[C:20]([NH2:23])(=[NH:22])[CH3:21]>>[CH3:21][C:20]1[N:22]=[CH:4][C:5]2[CH2:6][C:7](=[O:18])[NH:8][C:9]3[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][C:10]=3[C:11]=2[N:23]=1

Participants

3

Reactant 2

HCID 67170Acetamidine monohydrochlorideHCID 69923515HCID 69923515, compound

Product 1

HCID 23440980HCID 23440980, compoundYield 98%

Procedure

Analogous to Scheme 1, from 4-[(dimethylamino)methylene]-3,4-dihydro-7-methyl-1H-benzazepine-2,5-dione and acetamidine hydrochloride. Yield: 98%.

Sources & evidence

ORD record
ord-3e32e45135134bc8bca60be24c3f2298
Source dataset
uspto-grants-2004_02
Patent number
US06686352B2

Reaction notes

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