Acetamidine monohydrochloride → HCID 13133570, compound

HRID 2119972Notes

Reaction equation

HRID 2119972 reaction equation
CN([CH:4]=[C:5]1[C:11](=O)[C:10]2[CH:13]=[CH:14][CH:15]=[CH:16][C:9]=2[NH:8][C:7](=[O:17])[CH2:6]1)C.Cl.[C:19]([NH2:22])(=[NH:21])[CH3:20]>>[CH3:20][C:19]1[N:21]=[CH:4][C:5]2[CH2:6][C:7](=[O:17])[NH:8][C:9]3[CH:16]=[CH:15][CH:14]=[CH:13][C:10]=3[C:11]=2[N:22]=1

Participants

3

Reactant 2

HCID 67170Acetamidine monohydrochlorideHCID 669347634-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione

Product 1

HCID 13133570HCID 13133570, compoundYield 44%

Procedure

Analogous to Scheme 1, from 4-[(dimethylamino)methylene]-3,4-dihydro-1H-benzazepine-2,5-dione and acetamidine hydrochloride. Yield: 44%.

Sources & evidence

ORD record
ord-87caf5ac36ec49c5a24ab78b11a86faf
Source dataset
uspto-grants-2004_02
Patent number
US06686352B2

Reaction notes

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