Benzamidine, hydrochloride → HCID 23440951, compound

HRID 2119973Notes

Reaction equation

HRID 2119973 reaction equation
CN([CH:4]=[C:5]1[C:11](=O)[C:10]2[CH:13]=[CH:14][CH:15]=[CH:16][C:9]=2[NH:8][C:7](=[O:17])[CH2:6]1)C.Cl.[C:19]([NH2:27])(=[NH:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[C:20]1([C:19]2[N:26]=[CH:4][C:5]3[CH2:6][C:7](=[O:17])[NH:8][C:9]4[CH:16]=[CH:15][CH:14]=[CH:13][C:10]=4[C:11]=3[N:27]=2)[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1

Participants

3

Reactant 2

HCID 80289Benzamidine, hydrochlorideHCID 669347634-dimethylaminomethylene-3,4-dihydro-1H-benzo[b]azepine-2,5-dione

Product 1

HCID 23440951HCID 23440951, compoundYield 83%

Procedure

Analogous to Scheme 1, them 4-[(dimethylamino)methylene]-3,4-dihydro-1H-benzazepine-2,5-dione and benzamidine hydrochloride. Yield: 83%.

Sources & evidence

ORD record
ord-771bc08acf5e4d3e893928b97124e568
Source dataset
uspto-grants-2004_02
Patent number
US06686352B2

Reaction notes

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