HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentane → HCID 131720369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentane | HCID 8003 | — |
| Reactant | HCID 131720370 | HCID 131720370 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 131720369 | HCID 131720369 | — |
Reaction Steps
To 1.4 g (4.6 mmol) ((tetramethylcyclopentadienyl)dimethylsilyl) (2-methoxyphenyl)amine in diethyl ether was added dropwise 3.9 mL of 2.5 M butyl lithium (9.8 mmol) in hexane solvent. A white precipitate formed. Pentane was added to the mixture. The slurry was filtered and the solids washed with pentane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686488B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-eef03e2e18b04e6c819ade2f679863a2 |
| Source note | uspto-grants-2004_02 |