HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentane → HCID 131720371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentane | HCID 8003 | — |
| Reactant | HCID 131720372 | HCID 131720372 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 131720371 | HCID 131720371 | — |
Reaction Steps
((Tetramethylcyclopentadienyl)dimethylsilyl) (4-fluorophenyl)amine in diethyl ether solvent and butyl lithium 2.5 M in hexane solvent were combined in equivalent amounts. A white precipitate formed. Pentane was added to the slurry. The precipitate was filtered, washed with pentane and dried. 1H NMR (THF-d8) δ 7.28 (m, 2.0), 6.77 (m, 2), 3.27 (s, 2.7), 2.05 (s, 5.2), 2.01(s, 5.2), 0.44 (S, 4.6)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06686488B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-ec9250953d084743ac676cb0187a15e6 |
| Source note | uspto-grants-2004_02 |