Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Anisaldehyde sulfuric acid | HCID 21954228 | — |
Reaction Steps
Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06689398B2 |
|---|
| Source dataset | uspto-grants-2004_02 |
|---|
| ORD ID | ord-90ecde714b784ed2a46ee7c556fd8ada |
|---|
| Source note | uspto-grants-2004_02 |
|---|
