Thionyl Chloride → HCID 23437554, compound

Participants

Reaction Conditions

Reaction Steps

4-Dodecylsulfonylbenzoic acid (25.45 g, 71.8 mMole) was added to thionyl chloride (100 mL) together with 2 drops of dirnethylformarnide. The resulting mixture was heated to 60° C. for 3 hours. The solution was then cooled, concentrated under reduced pressure and co-evaporated with ethyl acetate (2×50 mL). The residual solid, assuming a quantitative yield, was taken on to the next step.

Provenance & Evidence