Ethylenediamine → HCID 135980093, compound

HRID 2120053Notes

Reaction equation

HRID 2120053 reaction equation
[CH:1]([N:4]([C:6]1[CH:7]=[C:8]([OH:14])[C:9](=[CH:12][CH:13]=1)[CH:10]=O)[CH3:5])([CH3:3])[CH3:2].[CH2:15]([NH2:18])[CH2:16][NH2:17]>>[CH:1]([N:4]([C:6]1[CH:7]=[C:8]([OH:14])[C:9](=[CH:12][CH:13]=1)[CH:10]=[N:17][CH2:16][CH2:15][N:18]=[CH:10][C:9]1[C:8](=[CH:7][C:6]([N:4]([CH3:5])[CH:1]([CH3:2])[CH3:3])=[CH:13][CH:12]=1)[OH:14])[CH3:5])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 3301EthylenediamineHCID 22664949HCID 22664949, compound

Product 1

HCID 135980093HCID 135980093, compound

Procedure

Synthesis and working up are carried out as in Example 9, starting from 500 mg (2.59 mmol) of 4-(N-isopropyl-N-methylamino)salicylaldehyde and 90 mg (1.5 mmol) of ethylenediamine.

Workup

  1. customSynthesis

Sources & evidence

ORD record
ord-a7331bcf8b6c45a89bee5b4294df549a
Source dataset
uspto-grants-2004_02
Patent number
US06689733B1

Reaction notes

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