2-Methylpropylenediamine → HCID 135819614, compound

HRID 2120056Notes

Reaction equation

[CH2:1]([N:3]([CH3:13])[C:4]1[CH:5]=[C:6]([OH:12])[C:7](=[CH:10][CH:11]=1)[CH:8]=O)[CH3:2].[NH2:14][CH2:15][C:16]([NH2:19])([CH3:18])[CH3:17]>>[CH2:1]([N:3]([C:4]1[CH:5]=[C:6]([OH:12])[C:7](=[CH:10][CH:11]=1)[CH:8]=[N:14][CH2:15][C:16]([CH3:18])([N:19]=[CH:8][C:7]1[C:6](=[CH:5][C:4]([N:3]([CH3:13])[CH2:1][CH3:2])=[CH:11][CH:10]=1)[OH:12])[CH3:17])[CH3:13])[CH3:2]

Participants

Reactant 2

HCID 131282-Methylpropylenediamine

HCID 22664951HCID 22664951, compound

Product 1

HCID 135819614HCID 135819614, compound

Procedure

Synthesis and working up are carried out as in Example 9, starting from 500 mg (2.79 mmol) of 4-(ethylmethylamino)salicylaldehyde and 117 mg (1.33 mmol) of 1,2-diamino-2-methylpropane.

Workup

customSynthesis

Sources & evidence

ORD record: ord-c37050a9c3524665965958b0d911aabd
Source dataset: uspto-grants-2004_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06689733B1

Reaction notes

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