2-Methylpropylenediamine → HCID 135819615, compound

HRID 2120057Notes

Reaction equation

[CH:1]([N:4]([C:6]1[CH:7]=[C:8]([OH:14])[C:9](=[CH:12][CH:13]=1)[CH:10]=O)[CH3:5])([CH3:3])[CH3:2].[NH2:15][CH2:16][C:17]([NH2:20])([CH3:19])[CH3:18]>>[CH:1]([N:4]([C:6]1[CH:7]=[C:8]([OH:14])[C:9](=[CH:12][CH:13]=1)[CH:10]=[N:15][CH2:16][C:17]([CH3:19])([N:20]=[CH:10][C:9]1[C:8](=[CH:7][C:6]([N:4]([CH3:5])[CH:1]([CH3:2])[CH3:3])=[CH:13][CH:12]=1)[OH:14])[CH3:18])[CH3:5])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 131282-Methylpropylenediamine

HCID 22664949HCID 22664949, compound

Product 1

HCID 135819615HCID 135819615, compound

Procedure

Synthesis and working up are carried out as in Example 9, starting from 500 mg (2.59 mmol) of 4-(N-isopropyl-N-methylamino)salicylaldehyde and 109 mg (1.23 mmol) of 1,2-diamino-2-methylpropane.

Workup

customSynthesis

Sources & evidence

ORD record: ord-36d983e8c7dd4b24aa23a0bd99f4684f
Source dataset: uspto-grants-2004_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06689733B1

Reaction notes

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