HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2,4-Dinitrobenzene → 2-(2,4-Dinitrophenoxy)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2,4-Dinitrobenzene | HCID 6 | — |
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 2-(2,4-Dinitrophenoxy)ethanol | HCID 76070 | 74.5% |
Reaction Steps
20.25 g (0.1 mole) of 2,4-dinitrochlorobenzene, 124 g (2 moles) of ethylene glycol, 82.93 g (0.6 mole) of potassium carbonate, and 600 ml of xylene were placed in a reaction vessel to be stirred by heating for 12 hours. The reacted solution was isolated by filtration, and the filtrate was concentrated. 17.0 g of 2-(2,4-dinitrophenoxy) ethanol was yielded by column purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689899B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-5b732e114435414e8cfe967ef7014979 |
| Source note | uspto-grants-2004_02 |