HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 86585895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | HCID 86585893 | HCID 86585893 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86585895 | HCID 86585895 | — |
Reaction Steps
To a solution of 1.0 equivalents of quinoxaline-2-carboxylic acid (1-benzyl-4-carbamimidoyl-7-fluoro-2-hydroxy-7-methyl-octyl)-amide in methylene chloride is added 1.0 equivalents of cyanogen bromide. The reaction is stirred at ambient temperature for approximately 15 hours. After standard aqueous work-up and extraction, followed by concentration and silica gel chromatography the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689886B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-0952e7603a324641acc8f65c7775f005 |
| Source note | uspto-grants-2004_02 |