HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 76550079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 57122273 | HCID 57122273 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 76550079 | HCID 76550079 | — |
Reaction Steps
In a manner similar to Example 3(i), by reacting 1.6 ml of tetrabutylammonium fluoride 1M/THF with 424 mg (0.71 mmol) of 6-{3-[3,4-bis-(tert-butyldimethylsilanyloxymethyl)benzyloxy]phenyl}-2-methylhepta-3,5-dien-2-ol in 15 ml of THF, after purification on a silica column (ethyl acetate 90-heptane 10), a yellow oil (m=206 mg; Y=79%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-bef80c324d734e95ba731005e7d808ec |
| Source note | uspto-grants-2004_02 |