HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 88055093, compound → HCID 23439804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 88055093 | HCID 88055093 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23439804 | HCID 23439804 | — |
Reaction Steps
350 mg of 5% rhodium/alumina are added to 750 mg (1.22 mmol) of ethyl 5-{3-[3,4-bis-(tert-butyldimethylsilanyloxymethyl)phenoxymethyl]phenyl}-hexa-2,4-dienoate in 50 ml of ethyl acetate. Hydrogen is bubbled through the medium for 1 hour 30 minutes. The mixture is then filtered on celite and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-61d50d196fff48a090ba228aab12751e |
| Source note | uspto-grants-2004_02 |