Acetic Acid → HCID 57112229, compound

Participants

Reaction Steps

In a manner similar to Example 8(k), by reacting 4.50 g (7.6 mmol) of 2-[6-(3-{2-[3-(tetrahydropyran-2-yl)-5-(tetrahydropyran-2-yloxy)phenyl]-vinyl}phenyl)-1,1-dimethylhexyloxy]tetrahydropyran with the solution of 100 ml of acetic acid, 50 ml of THF and 25 ml of water, and after purification on a silica column (ethyl acetate 50-heptane 50), beige crystals (m=1.23 g; Y=48%) are obtained. m.p.=98-100° C.

Provenance & Evidence