HCID 57112229, compound → HCID 9862889, compound

HRID 2120434Notes

Reaction equation

HRID 2120434 reaction equation
[OH:1][C:2]([CH3:25])([CH3:24])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:9]=[C:10]([CH:14]=[CH:15][C:16]2[CH:17]=[C:18]([OH:23])[CH:19]=[C:20]([OH:22])[CH:21]=2)[CH:11]=[CH:12][CH:13]=1>[Pd]>[OH:1][C:2]([CH3:25])([CH3:24])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:9]=[C:10]([CH2:14][CH2:15][C:16]2[CH:21]=[C:20]([OH:22])[CH:19]=[C:18]([OH:23])[CH:17]=2)[CH:11]=[CH:12][CH:13]=1

Participants

3

Reactant 1

HCID 57112229HCID 57112229, compound

Product 1

HCID 9862889HCID 9862889, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

In a manner similar to Example 9(a), by reacting 600 mg (1.76 mmol) of 5-{2-[3-(6-hydroxy-6-methylheptyl)phenyl]vinyl}benzene-1,3-diol with 60 mg of 10% palladium/carbon, pinkish crystals (m=368 mg; Y=61%) are obtained. m.p.=102-3° C.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-ac588b5a206945b88567fc48949b92f7
Source dataset
uspto-grants-2004_02
Patent number
US06689922B1

Reaction notes

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