HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 10133522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 87950611 | HCID 87950611 | — |
| Product | HCID 10133522 | HCID 10133522 | — |
Reaction Steps
In a manner similar to Example 59(h), by reacting 410 mg (0.7 mmol) of (3E,5E)-6-{3-[2-(3,4-bis-(tert-butyldimethylsilanyloxymethyl)phenyl)ethyl]-phenyl}-2-methylhepta-3,5-dien-2-ol (prepared in a manner similar to Examples 53(a-g)) with 2 ml (2 mmol) of a tetrabutylammonium fluoride solution (1M in THF), a colourless oil is obtained (m=230 mg; Y=96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-7543a3235406459eab35635ea2dfdb04 |
| Source note | uspto-grants-2004_02 |