HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium borohydride → HCID 9844459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium borohydride | HCID 4148881 | — |
| Reactant | HCID 86759341 | HCID 86759341 | — |
| Product | HCID 9844459 | HCID 9844459 | — |
Reaction Steps
In a manner similar to Example 53(e), by reacting 122 mg (0.26 mmol) of dimethyl 4-[3-((1E,3E)-5-ethyl-5-hydroxy-1-ethylhepta-1,3-dienyl)phenoxymethyl]phthalate (prepared in a manner similar to Examples 65(a-c)) with 17 mg (0.78 mmol) of lithium borohydride, a colourless oil is obtained (m=91 mg; Y=85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-3f7036122f704c8bacc8e807f4e50e88 |
| Source note | uspto-grants-2004_02 |