HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium borohydride → HCID 69685434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium borohydride | HCID 4148881 | — |
| Reactant | HCID 23439941 | HCID 23439941 | — |
| Product | HCID 69685434 | HCID 69685434 | — |
Reaction Steps
In a manner similar to Example 53(e), by reacting 397 mg (0.85 mmol) of dimethyl 4-[3-((E)-7-ethyl-7-hydroxy-1-methylnon-1-enyl)phenoxymethyl]phthalate (prepared in a manner similar to Examples 72(a-c)) with 55 mg (2.5 mmol) of lithium borohydride, a colourless oil is obtained (m=323 mg; Y=92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06689922B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-5107c92ceae84288bb57d26c4648280a |
| Source note | uspto-grants-2004_02 |