Lithium borohydride → HCID 10178767, compound

Participants

Reaction Steps

In a manner similar to Example 53(e), by reacting 390 mg (0.87 mmol) of dimethyl 4-[3-((E)-5-ethyl-5-hydroxy-1-methylhept-1-en-3-ynyl)phenoxymethyl]phthalate (prepared from the previous product in a manner similar to Example 64(d)) with 56 mg (2.6 mmol) of lithium borohydride, a colourless oil is obtained (m=248 mg; Y=72%).

Provenance & Evidence