Ammonium Chloride → HCID 87950066, compound

Participants

Reaction Steps

581 mg of 7-[5-(3,4-bis-benzoyloxymethylbenzyloxy)-2-methoxyphenyl]-3-ethylnona-4,6-dien-3-ol (0.89 mmol) are dissolved in 20 ml of a 2% potassium carbonate solution in methanol and then the reaction medium is stirred for 5 hours. After treating with a saturated ammonium chloride solution and extracting with ethyl acetate, the organic phases are combined, dried and concentrated under reduced pressure. The residue is purified by chromatography on a silica column. A yellow oil is obtained (m=284 mg; Y=72%).

Provenance & Evidence