Acryloyl chloride → HCID 22650072, compound

HRID 2120524Notes

Reaction equation

[O:1]1[CH:7]2[CH:2]1[C:3]([O:5][C:6]2([CH3:9])[CH3:8])=[O:4].[C:10](Cl)(=[O:13])[CH:11]=[CH2:12]>>[C:10]([O:1][CH:7]1[C:6]([CH3:8])([CH3:9])[O:5][C:3](=[O:4])[CH2:2]1)(=[O:13])[CH:11]=[CH2:12]

Participants

Reactant 2

HCID 13140Acryloyl chloride

HCID 22650065HCID 22650065, compound

Product 1

HCID 22650072HCID 22650072, compoundYield 87%

Procedure

The obtained 3-hydroxy-4,4-dimethyl-γ-butyrolactone was allowed to react with acrylyl chloride in the same manner as in Production Example 16 to thereby yield the title compound (yield: 87%).

Sources & evidence

ORD record: ord-4e0fcbad5b6d4c93a2e2ecd0a9198ce7
Source dataset: uspto-grants-2004_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06692889B1

Reaction notes

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