Acryloyl chloride → HCID 22650073, compound

HRID 2120525Notes

Reaction equation

[O:1]1[C:7]2([CH3:8])[CH:2]1[C:3]([O:5][C:6]2([CH3:10])[CH3:9])=[O:4].[C:11](Cl)(=[O:14])[CH:12]=[CH2:13]>>[C:11]([O:1][C:7]1([CH3:8])[C:6]([CH3:9])([CH3:10])[O:5][C:3](=[O:4])[CH2:2]1)(=[O:14])[CH:12]=[CH2:13]

Participants

Reactant 2

HCID 13140Acryloyl chloride

HCID 22650068HCID 22650068, compound

Product 1

HCID 22650073HCID 22650073, compoundYield 85%

Procedure

The obtained 3-hydroxy-3,4,4-trimethyl-γ-butyrolactone was allowed to react with acrylyl chloride in the same manner as in Production Example 16 to thereby yield the title compound (yield: 85%).

Sources & evidence

ORD record: ord-911c84fd3ce34469a48059a6c50c793a
Source dataset: uspto-grants-2004_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06692889B1

Reaction notes

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