4-tert-Butylchlorobenzene → HCID 23435198, compound

HRID 2120531Notes

Reaction equation

HRID 2120531 reaction equation
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([C:13]2[CH:18]=[CH:17][C:16]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:15][CH:14]=2)=O)=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[C:23]([C:27]1[CH:32]=[CH:31][C:30]([Cl:33])=[CH:29][CH:28]=1)([CH3:26])([CH3:25])[CH3:24]>>[Cl-:33].[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S+:11]([C:30]2[CH:31]=[CH:32][C:27]([C:23]([CH3:26])([CH3:25])[CH3:24])=[CH:28][CH:29]=2)[C:13]2[CH:18]=[CH:17][C:16]([C:19]([CH3:22])([CH3:21])[CH3:20])=[CH:15][CH:14]=2)=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 775944-tert-ButylchlorobenzeneHCID 184321184,4'-Sulfinylbis(tert-butylbenzene)

Product 1

HCID 23435198HCID 23435198, compound

Procedure

The end compound was synthesized as in Synthesis Example 4 except that bis(4-tert-butylphenyl) sulfoxide was used instead of the phenyl sulfoxide in Synthesis Example 4, 4-tert-butylchlorobenzene was used instead of the chlorobenzene, and the quantity of water for extraction was increased.

Workup

  1. extractionthe quantity of water for extraction
  2. temperaturewas increased

Sources & evidence

ORD record
ord-71ecfa8269194ac49962f9328a41bc3c
Source dataset
uspto-grants-2004_02
Patent number
US06692893B2

Reaction notes

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