HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 12990936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22062792 | HCID 22062792 | — |
| Reactant | HCID 86584107 | HCID 86584107 | — |
| Reactant | HCID 86584108 | HCID 86584108 | — |
| Product | HCID 12990936 | HCID 12990936 | — |
Reaction Steps
4-(2-phenoxy-ethyl)-benzoic acid (387 mg) was further reduced with LiAlH4, condensed with (R)-2-isocyanato-3-phenyl-propionate of formula 5 and hydrolyzed as described for example in Example 1, Steps 2-4, to yield about 550 mg of 2-[4-(2-phenoxy-ethyl)-benzyloxycarbonylamino]-3-phenyl-propionic acid 73, mp. 150.2-152.4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06693098B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-efe4e05f054347d7a66ec4136e17ebb9 |
| Source note | uspto-grants-2004_02 |