HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2120677Generated: October 31, 2026
Homoallyl bromide → N-(3-Buten-1-yl)phthalimide
https://huagongshe.com/reaction/2120677
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Homoallyl bromide | HCID 21241 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | N-(3-Buten-1-yl)phthalimide | HCID 339432 | — |
Reaction Steps
To a stirred solution of 4-bromo-1-butene (8-3, 20 g, 148 mmol) in DMF (150 mL) was added potassium phthalimide (8-4, 25 g, 133 mmol) and the mixture stirred for 18 hours at 70° C. After cooling to RT, the mixture was diluted with ether, washed with water and brine, dried over MgSO4, and concentrated to give 8-5 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06693101B2 |
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| Source dataset | uspto-grants-2004_02 |
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| ORD ID | ord-8b297bcbe2244dc8ae54dbe23856ff43 |
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| Source note | uspto-grants-2004_02 |
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