Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69883122 | HCID 69883122 | — |
| Product | HCID 10111379 | HCID 10111379 | — |
Reaction Steps
To a solution of 8-14 (0.50 g, 1.36 mmol) in ethanol (10 mL) was added 1N NaOH (1.5 mL), and the mixture stirred at 50° C. for 30 minutes, then concentrated. The residue was chromatographed on silica gel (25:10:1:1 to 15:10:1:1 EtOAc/EtOH/NH4OH/H2O) to give 8-15 as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06693101B2 |
|---|
| Source dataset | uspto-grants-2004_02 |
|---|
| ORD ID | ord-dd6b5e3211ac4f8ba682bd79072e6057 |
|---|
| Source note | uspto-grants-2004_02 |
|---|
