Acetone → HCID 9861056, compound
Reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([N+:14]([O-:16])=[O:15])[CH:9]=2)=[CH:4][C:3]=1[CH:17]([OH:19])[CH3:18].[CH3:20][C:21]([CH3:23])=O>>[N+:14]([C:10]1[CH:9]=[C:8]([C:5]2[CH:6]=[CH:7][C:2]3[NH:1][C:21]([CH3:23])([CH3:20])[O:19][CH:17]([CH3:18])[C:3]=3[CH:4]=2)[CH:13]=[CH:12][CH:11]=1)([O-:16])=[O:15]Participants
3
Procedure
Prepared from 1-(4-amino-3′-nitro-biphenyl-3-yl)-ethanol and acetone in the same fashion as that of Example 4. Yellow solid: mp 188-189° C.; Anal. Calc. For C17H18N2O3.0.35H2O: C, 67.02; H, 6.19; N, 9.20. Found: C, 66.7; H, 5.89; N, 9.03.
Sources & evidence
- ORD record
- ord-5364075a5a0444f29e79edd37fa97bad
- Source dataset
- uspto-grants-2004_02
- Patent number
- US06693103B2
Reaction notes
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