2,4,6-Trimethylaniline → HCID 178425519, compound

Participants

Reaction Steps

A 100-mL round-bottom flask equipped with a nitrogen inlet and an internal fritted-glass filter is charged with phthalonitrile (2.56 g, 20.0 mmol) and ethanol (50 mL). 2,4,6-Trimethylaniline (5.68 g, 42.0 mmol, 2.1 eq.) and iron(II) chloride (2.54 g, 20.0 mmol) are added to the flask, and the mixture is stirred at room temperature under nitrogen for 1 h.

Provenance & Evidence