HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 23436676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 86588814 | HCID 86588814 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23436676 | HCID 23436676 | 88.2% |
Reaction Steps
A flask containing 19.45 grams (90.74 mmol) of 2-methyl-2-adamantylcyclopentadiene was charged with 30 mL acetone, 100 mL methanol, and 10 mL pyrrolidine (120 mmol). The solution formed a yellow precipitate over 96 hours which was collected by suction filtration and rinsed with 50 mL methanol. The material was dried in vacuo to provide 20.36 grams of product as a yellow powder (88.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06693153B2 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-d4ad51dda8fc470585faff5e313ebe51 |
| Source note | uspto-grants-2004_02 |