HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131724348, compound → HCID 131724347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131724348 | HCID 131724348 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131724347 | HCID 131724347 | 192.3% |
Reaction Steps
A solution of 590 mg of CBZ-D-Trp-Lys(OtBu)-OtBu was hydrogenated at 50 PSI for 2.5 hours in 50 mL of methanol with 100 mg of 10% palladium on carbon catalyst. The catalyst was then filtered off and the solvent evaporated to yield 466 mg (95%) of D-Trp-Lys(BOC)-OtBu (see Scheme 2A, reactants 9→8).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06696418B1 |
| Source dataset | uspto-grants-2004_02 |
| ORD ID | ord-b6dce41e253f4f3fbced8665d4378085 |
| Source note | uspto-grants-2004_02 |